Preparation process of leak protection plugging agent along with drilling based on control of monomer concentration
A technology of monomer concentration and preparation process, which is applied in the direction of drilling composition, chemical instruments and methods, etc., can solve the problems of delaying drilling time, reducing drilling efficiency, and consuming a lot of time, so as to reduce production costs and increase production efficiency , Facilitate the effect of processing
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[0029] The invention relates to a preparation process of an anti-leakage plugging agent while drilling based on controlling the concentration of a monomer, comprising the following steps:
[0030] (a) AM and AMPS are purified for subsequent use;
[0031] (b) Weigh a certain amount of AA and hydrolyze it, and move it into a reaction vessel placed in a super constant temperature water bath;
[0032] (c) adding a certain amount of cross-linking agent;
[0033] (d) adding a certain amount of AM and AMPS, and the total monomer concentration is 14.3% to 18.2% by mass, and adjusting the pH value of the reaction system to 7 with 10% sodium hydroxide solution;
[0034] (e) After exhausting oxygen with an inert gas and stirring for about a period of time, add the initiator;
[0035] (f) Adjust the temperature to the reaction temperature, and polymerize for a certain period of time to obtain the target product.
[0036] In the step (a), AM and AMPS are purified by ethanol.
[0037] In t
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