Method for preparing silver nanowire in hydrophobic phase

A nanowire and hydrophobic phase technology, applied in nanotechnology and other directions, can solve the problem that silver nanowires cannot be uniformly dispersed, and achieve the effect of expanding the application field and simple process

Active Publication Date: 2015-10-28
山东利特纳米技术有限公司
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  • Abstract
  • Description
  • Claims
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Problems solved by technology

[0004] In view of the above-mentioned deficiencies in the prior art, the present invention provides a method for preparing silver nanowires in a hydrophobic phase. The silver nanow

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  • Method for preparing silver nanowire in hydrophobic phase
  • Method for preparing silver nanowire in hydrophobic phase
  • Method for preparing silver nanowire in hydrophobic phase

Examples

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Example Embodiment

[0028] Example 1

[0029] At room temperature, mix 300 mg of silver bromide, 3 mg of cupric chloride and 30 g of oleylamine, stir and fully dissolve to obtain a mixed solution, raise the temperature of the mixed solution to 160°C for 6 hours, then cool to room temperature to obtain a reaction solution, and use Wash with cyclohexane, filter, and dry to obtain silver nanowires. The silver nanowire that present embodiment makes (see figure 1 ), with an average diameter of 60 nm and an average length of 10 μm.

Example Embodiment

[0030] Example 2

[0031] At room temperature, mix 300 mg of silver bromide, 3 mg of copper sulfate and 30 g of oleylamine, stir to dissolve fully to obtain a mixed solution, raise the temperature of the mixed solution to 160°C for 6 h, then cool to room temperature to obtain a reaction solution, and use Wash with cyclohexane, filter, and dry to obtain silver nanowires. The silver nanowire that present embodiment makes (see figure 2 ), with an average diameter of 55 nm and an average length of 15 μm.

Example Embodiment

[0032] Example 3

[0033] At room temperature, mix 300 mg of silver bromide, 3 mg of copper oxide and 30 g of oleylamine, stir to dissolve fully to obtain a mixed solution, raise the temperature of the mixed solution to 160°C for 6 h, then cool to room temperature to obtain a reaction solution, and use Wash with cyclohexane, filter, and dry to obtain silver nanowires. The silver nanowire that present embodiment makes (see image 3 ), with an average diameter of 67 nm and an average length of 10 μm.

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Abstract

The invention discloses a method for preparing a silver nanowire in the hydrophobic phase. The method comprises the following steps: mixing silver bromide, copper salt and a solvent at the room temperature; stirring to be fully dissolved to obtain a mixed solution; heating the mixed solution up to 100-267 DEG C for 1-24 hours' reaction; then cooling to the room temperature to obtain a reaction solution; and washing, filtering and drying the reaction solution to obtain the silver nanowire. The method is simple in process, and only requires mixing of the three raw materials and heating for reaction without shaking, ultrasonic and other operation methods. The prepared silver nanowire has hydrophobic groups on the surface, and can be effectively and uniformly dispersed in hydrophobic solvents and materials, so that the application field of the silver nanowire is expanded.

Description

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Claims

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Application Information

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Owner 山东利特纳米技术有限公司
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