Active carbon material derived based on green soy bean shells as well as preparation method and application of active carbon material
A technology of activated carbon and edamame shell, applied in the field of materials, achieves the effects of high yield, mild working conditions and simple operation
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Example Embodiment
[0036] Embodiment 1, the preparation of activated carbon material derived from edamame hulls
[0037] The preparation method of the activated carbon material derived from edamame hulls, the specific steps are as follows:
[0038](1) Put the edamame shell powder with a particle size of 60 mesh in a tube furnace, under the protection of argon, raise the temperature at a rate of 5 °C / min to 200 °C for 1 hour, and then continue to heat up at a rate of 5 °C / min to Insulate at 400°C for 1 hour, then raise the temperature at a rate of 5°C / min to 800°C for 3 hours, and finally cool to room temperature to obtain a crude carbon material precursor derived from edamame hulls;
[0039] (2) Soak the crude carbon material precursor prepared in step (1) with a hydrochloric acid solution with a mass fraction of 10% for 1 hour, repeatedly suction filter and wash, and dry at 80° C. for 10 hours to obtain a crude carbon material;
[0040] (3) The coarse carbon material prepared in step (2) is
Example Embodiment
[0042] Embodiment 2, the preparation of activated carbon material derived from edamame hulls
[0043] The preparation method of the activated carbon material derived from edamame hulls, the specific steps are as follows:
[0044] (1) Put the edamame shell powder with a particle size of 40 mesh in a tube furnace, under the protection of argon, raise the temperature at a rate of 2°C / min to 200°C for 1 hour, and then continue to heat up at a rate of 2°C / min to Insulate at 400°C for 1 hour, then raise the temperature at a rate of 2°C / min to 800°C for 3 hours, and finally cool to room temperature to prepare a crude carbon material precursor;
[0045] (2) Soak the coarse carbon material precursor prepared in step (1) with 15% acetic acid solution for 1 hour, repeatedly suction filter and wash, and dry at 80° C. for 10 hours to obtain a coarse carbon material;
[0046] (3) Mix the coarse carbon material prepared in step (2) with KOH at a mass ratio of 2:1, and after fully grindin
Example Embodiment
[0048] Embodiment 3, the preparation of activated carbon material derived from edamame hulls
[0049] The preparation method of the activated carbon material derived from edamame hulls, the specific steps are as follows:
[0050] (1) Put the edamame shell powder with a particle size of 30 mesh in a tube furnace, under the protection of argon, raise the temperature at a rate of 3°C / min to 200°C for 1 hour, and then continue to heat up at a rate of 3°C / min to Insulate at 400°C for 1 hour, then raise the temperature at a rate of 3°C / min to 800°C for 3 hours, and finally cool to room temperature to prepare a crude carbon material precursor;
[0051] (2) Soak the coarse carbon material precursor prepared in step (1) with 20% sulfuric acid solution for 1 hour, repeatedly suction filter and wash, and dry at 80° C. for 10 hours to obtain a coarse carbon material;
[0052] (3) The coarse carbon material prepared in step (2) is mixed with KOH at a mass ratio of 3:1, after being full
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