Method for preparing high-density fused magnesite by reburning electric smelting composite process

A composite process, the technology of fused magnesia, which is applied in the field of fused magnesia smelting, can solve the problems of low density of fused magnesia, and achieve the effects of reducing porosity, increasing density, and remarkable exhaust effect

Pending Publication Date: 2020-04-28
HAICHENG CITY ZHONGHAO MAGNESIUM CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0004] The present invention aims to overcome the deficiency of low density of fused magnesia in the prior a

Method used

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  • Method for preparing high-density fused magnesite by reburning electric smelting composite process

Examples

Experimental program
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Effect test

Example Embodiment

[0018] Example 1

[0019] Calcined 10 kg of magnesite ore with a mass percentage of 45% by mass in a high temperature shaft kiln at 1450°C for 4 hours to obtain recalcined magnesia; crush the recalcined magnesia in a jaw crusher to a particle size of 60- 80mm block; melt the block with a particle size of 60-80mm in an electric arc furnace at 2650℃ (the diameter of the graphite electrode of the arc furnace is 300mm, the bending strength of the graphite electrode is 10MPa, the compressive strength of the graphite electrode is 20MPa, and the ash content of the graphite electrode is 0.5 %), the submerged arc melting time is 10h; the molten fused magnesia lumps are naturally cooled for 7 days; the cooled fused magnesia lumps are manually broken to obtain the molten fused magnesia lumps.

[0020] According to GB / T2997-2000, the volume density and porosity of the test sample are measured; the crystal grain size of the sample is measured under the Zeiss-ΣIGMA-HD scanning electron microscope

Example Embodiment

[0021] Example 2

[0022] Calcined 10kg of magnesite ore with a mass percentage of 46% magnesia in a high temperature shaft kiln at 1500°C for 4 hours to obtain recalcined magnesia; crush the recalcined magnesia in a jaw crusher to a particle size of 70- 90mm block material; melt the block material with a particle size of 70-90mm in an electric arc furnace at 2750℃ (the diameter of the graphite electrode of the arc furnace is 300mm, the bending strength of the graphite electrode is 10MPa, the compressive strength of the graphite electrode is 20MPa, and the ash content of the graphite electrode is 0.5 %), the submerged arc melting time is 10h; the molten fused magnesia lumps are naturally cooled for 8 days; the cooled fused magnesia lumps are broken manually to obtain the molten fused magnesia lumps.

[0023] According to GB / T2997-2000, the volume density and porosity of the test sample are measured; the crystal grain size of the sample is measured under the Zeiss-ΣIGMA-HD scanning e

Example Embodiment

[0024] Example 3

[0025] Calcined 10kg of magnesite ore with a mass percentage of 47% magnesia in a high temperature shaft kiln at 1600°C for 4 hours to obtain recalcined magnesia; crush the recalcined magnesia in a cone crusher to produce a particle size of 80-100mm The block material with a particle size of 80-100mm is melted in an electric arc furnace at 2750℃ (the diameter of the graphite electrode of the arc furnace is 300mm, the bending strength of the graphite electrode is 10MPa, the compressive strength of the graphite electrode is 20MPa, and the ash content of the graphite electrode is 0.5% ), the submerged arc melting time is 10h; the molten fused magnesia lumps are naturally cooled for 8 days; the cooled fused magnesia lumps are manually broken to obtain the molten fused magnesia lumps.

[0026] According to GB / T2997-2000, the volume density and porosity of the test sample are measured; the crystal grain size of the sample is measured under the Zeiss-ΣIGMA-HD scanning el

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Abstract

The invention relates to a method for preparing high-density fused magnesite by a reburning and electric smelting composite process. The preparation process comprises the steps of reburning, crushing,melting, cooling and lump breaking. The method has the beneficial effects that magnesite is reburnt at the high temperature of 1400-1800 DEG C, so that CO2 gas escapes completely, the porosity of thematerial is reduced, and the slag corrosion resistance is enhanced. The fused magnesite is obtained by smelting dead burned magnesia blocks with the particle size of 50-100 mm, and due to the fact that the dead burned magnesia is blocky, the exhaust effect is remarkable, and low-melting-point impurities are sublimated and converted into gaseous impurities to be exhausted more smoothly. The fusedmagnesite produced by the method is beneficial to increase of the content of magnesium oxide, enhancement of the densification degree and improvement of the slag resistance.

Description

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Claims

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Application Information

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Owner HAICHENG CITY ZHONGHAO MAGNESIUM CO LTD
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