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2 results about "Carbonation" patented technology

Carbonation is the chemical reaction of carbon dioxide to give carbonates, bicarbonates, and carbonic acid. In chemistry, the term is sometimes used in place of carboxylation, which refers to the formation of carboxylic acids.

Method for preparing hetero-atom doped porous carbon material through carbonation of biomass under assistance of molten salt

InactiveCN105314622ALarge specific surface areaImprove conductivityIn situ dopingPorous carbon
The invention provides a method for preparing a hetero-atom doped porous carbon material through carbonation of biomass under the assistance of molten salt. The method comprises the following steps: uniformly mixing biomass powder, the molten salt and a hetero-atom doped compound to obtain a product A, wherein the molten salt contains LiCl and KCl, the mass of LiCl accounts for 59 percent of that of the molten salt, and the mass of KCl accounts for 59 percent of that of the molten salt; putting the product A in a pipe furnace; carrying out high-temperature calcination; cleaning with distilled water to remove the molten salt and obtain the final product, namely the hetero-atom doped porous carbon material. The method has the advantages that the biomass is taken as a raw material, and the molten salt containing hetero-atoms is taken as a carbonization medium, so that the hetero-atoms can be introduced into the skeleton of the carbon material during the pyrolysis and carbonization process of the biomass synchronously and controllably, and the hetero-atom in-situ doped porous carbon material is obtained finally. Compared with the conventional doping method, the method provided by the invention have the advantages that the steps are simple; the cost is low; the operation is easy; the reactant purity is high; the application prospect is relatively good.
Owner:HARBIN ENG UNIV

Method for preparing coarse granularity chromium carbide powder

ActiveCN108046259AMeet wear resistanceCorrosiveCarbon compoundsChemical industryAdhesiveWear resistant
The invention discloses a method for preparing coarse granularity chromium carbide powder capable of simplifying the process, saving the energy consumption, improving the rate of qualified products ina milling process and well meeting requirements of preparation of wear-resistant, corrosion-resistant, high-temperature oxidation resistant novel materials in industries such as hard-face materials,flux-cored wires, high temperature alloys and the like. The method comprises the following steps: burdening chromium sesquioxide powder and carbon, and adding an adhesive to be uniformly mixed; molding with a press after uniform mixing; placing the molded material block in a high-temperature vacuum induction heating furnace graphite crucible, vacuumizing, performing power-on heating and raising the temperature, and maintaining the vacuum degree to be within 200-400Pa; carrying out a vacuum carbonation reaction between the chromium sesquioxide powder and carbon to produce chromium carbide, andcontrolling the carbonation reaction temperature to be 1350-1550 DEG C, wherein the carbonation reaction time is 8-15 hours; enabling the vacuum degree to be less than 100Pa, filling the furnace withargon after the carbonation reaction is completed, controlling the pressure in the furnace to be 40-80kPa, and increasing the heating power to melt the chromium carbide sintered body so as to obtain achromium carbide ingot; crushing the chromium carbide ingot into particles with the granularity of less than 10mm by using a mechanical method, milling by an impact crusher, and passing through a 60-mesh sieve, thereby obtaining the coarse granularity chromium carbide powder.
Owner:锦州市金属材料研究所
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