Preparation method of ginsenoside Rg1
A technology of ginsenosides and total saponins, applied in the directions of steroids, organic chemistry, etc., can solve the problems of high cost and difficult industrialized production, etc.
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Embodiment 1
[0068] The Panax notoginseng total saponins obtained by the extraction of Panax notoginseng were dissolved in water, filtered, the filtrate passed through the HPD-400A macroporous adsorption resin column, washed with water, the eluent was discarded, eluted with 20% ethanol, the eluate was collected, concentrated, and dried. Dissolve the dry matter in water, filter, and pass the filtrate through the HPD-400A macroporous adsorption resin column, wash with water, discard the eluent, then elute with 10% ethanol, discard the eluent, elute with 20% ethanol again, collect The eluate was concentrated and dried to obtain ginsenoside Rg 1 The crude product is extracted by adding organic solvent acetone, the extract is filtered, the filtrate recovers the solvent to dryness, and the residue is dried to obtain ginsenoside Rg 1 .
[0069] The method for extracting total saponins from Panax notoginseng is prepared according to existing patent documents or scientific documents.
[0070] The...
Embodiment 2
[0072] Take the total saponins extracted from ginseng and dissolve in water, filter, pass the filtrate through HPD-400 macroporous adsorption resin column, wash with water, discard the eluent, elute with 60% ethanol, collect the eluate, concentrate, dry, add water to the dry matter Dissolve, filter, pass the filtrate through HPD-400 macroporous adsorption resin column, wash with water, discard the eluent, then elute with 50% ethanol, discard the eluent, then elute with 60% ethanol, collect the eluate , concentrated and dried to obtain ginsenoside Rg 1 The crude product is extracted by adding organic solvent butanone, the extract is filtered, the filtrate recovers the solvent to dryness, and the residue is dried to obtain ginsenoside Rg 1 .
[0073] The extraction method of total ginseng saponins is prepared according to existing patent documents or scientific documents.
[0074] The above-mentioned ginsenoside Rg 1 As pharmaceutical raw materials, it can be prepared into ph...
Embodiment 3
[0076] Extract the total saponins obtained from American ginseng, dissolve them in water, filter, pass the filtrate through a HPD-300 macroporous adsorption resin column, wash with water, discard the eluent, elute with 25% ethanol, collect the eluate, concentrate, dry, and dissolve the dry matter in water , filtered, the filtrate was passed through a HPD-300 macroporous adsorption resin column, washed with water, and the eluent was discarded, then eluted with 15% ethanol, the eluent was discarded, and then eluted with 25% ethanol, and the eluate was collected. Concentrate and dry to get ginsenoside Rg 1 The crude product is extracted by adding organic solvents n-butanol, ethanol, and methanol, the extract is filtered, the filtrate is recovered from the solvent to dryness, and the residue is dried to obtain ginsenoside Rg 1 .
[0077] The extraction method of total saponins of American ginseng is prepared according to existing patent documents or scientific documents.
[0078...
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