Binder for resin composite material and preparation method of binder

[0032] The preparation method of the binder for the resin composite material comprises the following steps:

[0033] Step 1: Add 20.8-22.7 parts of phenolic alcohol head and 0.8-1.6 parts of catalyst into a high-pressure reactor equipped with a stirrer and a thermometer. After nitrogen replacement for 3 times, start vacuuming to gauge pressure -0.15MPa, and then heat up to 130- Dehydration starts at 135°C for 1-2 hours, and the constant temperature is around 125°C. Start to feed the cyclic monomer into the reactor, and feed 291.6-311.4 parts of the cyclic monomer into the reactor, and control the pressure to be less than 0.45MPa. After the passage, keep the temperature at 125-140°C for aging to negative pressure, cool down and discharge, The prepared polyether was obtained.

[0034]Step 2: Add the finished polyether into the reaction kettle, and heat up to 65-80°C by using a water bath. Prepare 6.1-8.3 parts of reducing agent, 4.7-6.5 parts of chain transfer agent, 137.8-145...

[0036] A binder for resin composite materials, which is formed by polymerizing the following components, the total mass of raw materials is 1000 parts, and each component includes: 21.5 parts of 2-methoxy-6-(2-propenyl)-phenol , 305 parts of propylene oxide, 1.2 parts of boron trifluoride, 140 parts of poly-1,2-propylene glycol, 7.0 parts of a composition of sodium dithionite and sodium metabisulfite with a mass ratio of 1:1, 6.2 parts of ammonium persulfate, mercaptopropyl 3.3 parts of acid, 26.5 parts of 3-(methacryloyloxy)propyltrimethoxysilane, 9.5 parts of diethanolamine, and the rest is water, with a total mass of 1000 parts.

[0037] The preparation method of the binder for the resin composite material comprises the following steps:

[0038] Step 1: Add 21.5 parts of 2-methoxy-6-(2-propenyl)-phenol and 1.2 parts of boron trifluoride into a high-pressure reactor equipped with a stirrer and a thermometer, and start vacuuming after nitrogen replacement for 3 times To the ...

[0040] Examples 2-6: According to the method of the present invention, according to the raw material composition and step parameters in Tables 1 and 2, binders for resin composite materials were prepared.

[0041] Table 1

[0042]

[0043]

[0044] Table 2

[0045]