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11 results about "Chemical products" patented technology

Method for extracting multiple chemical products from coal-tar oil

ActiveCN101139527AIncrease added valueQuality improvementTar working-up by water removalTar working-up by distillationAnthraceneHigh concentration
The invention discloses a method for extracting a plurality of chemicals from a coal tar, which comprises such procedures as heating the coal tar to 120-130 DEG C, dehydrating, fore running, separating, fine rectifying, and heavy-oil distilling, and getting 95 naphthalene, methyl naphthalene, anthracene oil, asphalt and heavy oil. The invention is of simple process, easy operation, rectifies coal tar several times; the extracted chemical products are of steady quality, the naphthalene is of high concentration, and the asphalt is of good quality. The invention is of low energy consumption, hence improves better the added value in processing coal tar in China.
Owner:ZHEJIANG MEIYANG INTL PETROCHEMICAL MEDICINE DESIGN CO LTD

Method for preparing pirfenidone

InactiveCN102558040AReduce energy consumptionSimple and fast operationOrganic chemistryPurification methodsChemical products
The invention discloses a method for preparing pirfenidone, comprising the following steps: subjecting 2-amino-5-methylpyridine which is a starting material to inverse diazotization and hydrolysis, extracting with extraction solvent, and recrystallizing with recrystallization solvent to obtain 2-hydroxy-5-methylpyridine; heating the 2-hydroxy-5-methylpyridine together with iodobenzene in the presence of anhydrous potassium carbonate and active copper to subject the 2-hydroxy-5-methylpyridine and the iodobenzene to nucleophilic substitution reaction to generate a target compound which is the crude pirfenidone; and recrystallizing the crude pirfenidone for one time for purification with recrystallization solvents which are ethyl acetate and anhydrous ethyl alcohol to obtain the pure pirfenidone. Compared with the prior art, the method for preparing the pirfenidone has the characteristics that: the 2-amino-5-methylpyridine which is the starting material is a commercial chemical product, is cheap and is easy to get, the inverse diazotization replaces the conventional diazotization reaction so that the operation is simple, and the purification methods of the 2-hydroxy-5-methylpyridine and the end product which is the pirfenidone are easy to operate and have high yield. The method for producing the pirfenidone consumes less energy, and the production cost is lowered due to the adoption of the method.
Owner:CISEN PHARMA

Synthesis method of 2-(2-chloroethoxy) acetic acid

InactiveCN101844978AZero costSimple and fast operationOrganic compound preparationCarboxylic compound preparationAcetic acidOrganic solvent
The invention relates to a synthesis method of 2-(2-chloroethoxy) acetic acid, which belongs to the technical field of the preparation and the application of fine chemical engineering products. The invention particularly belongs to the synthesis method of 2-(2-chloroethoxy) acetic acid. The invention uses 2-chloroethoxy ethanol as starting materials, uses water as solvents, and uses nitric acid for direct oxidization to obtain products. The reaction process is shown as the accompanying drawing. The invention adopts water as the solvents, and uses the nitric acid as oxidizing agents for efficiently oxidizing the 2-chloroethoxy ethanol into corresponding acids. The method has the advantages of simple operation, low price of raw materials, easy acquisition of raw materials, simple requirement on equipment, simple after treatment and the like. In addition, the use of the organic solvent has nearly zero cost, and the invention conforms to the environmental protection industrial production requirements, so the invention has wide application prospects.
Owner:NANKAI UNIV

Inert chemical product charging bucket cleaning device

The invention relates to a cleaning device for chemical products, in particular to an inert chemical product charging bucket cleaning device. According to the technical purposes of the inert chemicalproduct charging bucket cleaning device, the cleaning effect is good, operation is easy and convenient, and injuries to human bodies are small. In order to achieve the technical purposes, the inert chemical product charging bucket cleaning device is provided and comprises supporting legs and the like; a first supporting plate is horizontally placed on the tops of the left and right side supportinglegs; a cleaning mechanism is installed in the middle of the bottom of the first supporting plate; and a second supporting plate is connected to the position, close to the upper portion, of the bottom between the left and right side supporting legs, and is provided with an overturning and tipping mechanism. According to the inert chemical product charging bucket cleaning device, due to mutual cooperation of the cleaning mechanism and the overturning and tipping mechanism, recycled charging barrels are cleaned, and meanwhile, by means of optimization of an auxiliary mechanism and a secondary treatment mechanism, the effects that the cleaning effect is good, operation is easy and convenient, and injuries to human bodies are small are achieved.
Owner:饶胜智

Fixed-bed pure-oxygen continuous gasification device and process adaptable to diversified coals

ActiveCN105542860AImprove decomposition rateHigh effective gas contentChemical industryGasification processes detailsAdditive ingredientFixed bed
The invention relates to a fixed-bed pure-oxygen continuous gasification device and process adaptable to diversified coals. According to the device and the process, CO2, pure oxygen and superheated steam serve as gasifying agents and subject to a gasification reaction with feed coal in a fixed-bed pure-oxygen continuous gasifier, so as to generate gasified coal gas; the gasified coal gas enters a dust remover so as to remove solid particles from the gasified coal gas, and a water cooler is arranged at the upper part of the efficient dust remover and is used for recovering part of sensible heat from the gasified coal gas; the gasified coal gas subjected to dust removal enters a heat-pipe heat exchanger for heat recovery, and low-pressure steam is a byproduct; and low-temperature gasified coal gas enters a low-pressure coal gas scrubbing tower for final cooling and dust removal, and scrubbed water gas is connected and conveyed to a gas tank. The content of CO and H2 in the gasified coal gas can reach 80% or more, the ratio range of adjustment of CO among ingredients of the coal gas is 40-65%, the ratio range of adjustment of H2 among the ingredients of the coal gas is 5-40%, and the gasified coal gas can serve as raw material gas of a variety of chemical products through being subjected to further deep treatment by processes such as conversion and purification.
Owner:河南顺达新能源科技有限公司
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