The invention discloses a sample for detecting the dispersion state of filler. The sample is used for detecting the dispersion state of the filler in a
polymer composite. The sample comprises the
polymer composite and a loading device for applying a load to the
polymer composite, wherein the polymer composite deforms through loading by the loading device and is located on the loading device through a locating mechanism, so that the polymer composite remains deformed and forms a sample core with the loading device; the sample core is wrapped in a cured body formed by curing of a curing agent. The invention further provides a preparation method. The preparation method comprises the following steps: applying the load to the polymer composite for deformation, keeping deformation of the polymercomposite on the loading device by the locating mechanism to form the sample core, and curing the sample core. The invention also provides a use method. The use method comprises the following steps:
slicing the sample and observing the slice under an atomic force
microscope. The shape and dispersion state of the filler in the composite under different load conditions can be tested simply and effectively.