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14 results about "Imide" patented technology

In organic chemistry, an imide is a functional group consisting of two acyl groups bound to nitrogen. The compounds are structurally related to acid anhydrides, although imides are more resistant toward hydrolysis. In terms of commercial applications, imides are best known as components of high-strength polymers, called polyimides.

Preparation method of styrene-maleic anhydride-nitrophenyl maleimide terpolymer

InactiveCN109021155AShort processSimple post-processingImidePolymer science
The invention discloses a styrene-maleic anhydride-nitrophenyl maleimide terpolymer and a preparation method thereof. The terpolymer is characterized by comprising the following components by weight percentage: 50-90 parts of styrene, 1-20 parts of maleic anhydride, and 10-30 parts of nitrophenyl maleimide. The glass transition temperature is 150-200DEG C, a bulk polymerization way is employed forpreparation, firstly part of the styrene is added into a reaction kettle, then a styrene solution with dissolved maleic anhydride and nitrophenyl maleimide is added dropwise into the reaction kettle,the temperature of the reaction kettle is 90-140DEG C, and the pressure is atmospheric pressure, after reaction to a certain degree, high temperature vacuum devolatilization is carried out to obtainthe terpolymer. Compared with the prior art, the preparation method provided by the invention has the advantages of simple process, no waste water, and environment-friendly production process, and theprepared product has high purity, and is suitable for use as a low odor and low emission heat resistant agent for vehicle ABS and household appliance ABS.
Owner:JIAXING HUAWEN CHEM CO LTD

Low melt viscosity imide oligomers and polyimides therefrom

ActiveUS7605223B1Easy to prepareImprove performanceAdhesivesImideOligomer
The present invention relates to novel imide oligomer compositions, polyimides formed therefrom, and methods for making and using the same. In particular, the invention relates to novel polyimide oligomers comprising 3,3′,4,4′-benzophenone tetracarboxylic dianhydride (BTDA), 2-(3,4-dicarboxy phenyl)-1-phenylacetylene anhydride (PE), and a mixture of 1,3-diaminobenzene and 4,4′-(1,3-phenylenediisopropylidene) bisaniline. The polyimide oligomers demonstrate low melt viscosity (these resins are melt processable) while retaining exceptional thermo-oxidative stability, high glass transition temperature, and good mechanical properties in the cured state.
Owner:PERFORMANCE POLYMER SOLUTIONS

Triarylmethane compound and its preparation method and use

InactiveCN103275060ALow costLow photoelectric conversion performanceLight-sensitive devicesOrganic chemistryCyanoacetic acidEthylic acid
The invention discloses a triarylmethane compound and its preparation method and use. The preparation method comprises the following steps that 1, R2-CHO and R1-H undergo a reaction to produce a compound I; and 2, the compound I and a Vilsmeier reagent undergo a reaction to produce a compound II; and the compound II and cyanoacetic acid undergo a reflux reaction in an acetic acid solution to produce the triarylmethane compound; or 3, the compound I and N-bromosuccinimide undergo a bromination reaction to produce a compound III; the compound III and (OH)2B-R3-CHO undergo a reflux reaction in methylbenzene or chloroform to produce a compound IV; and the compound IV and cyanoacetic acid undergo a reflux reaction in an acetic acid solution to produce the triarylmethane compound. The triarylmethane compound is used as a photosensitive dye and is used for preparation of a dye-sensitized solar cell material. The triarylmethane compound has wide and cheap raw material sources. The preparation method has simple processes and a low cost, can be industrialized and can be used as a novel dye-sensitized solar cell material.
Owner:CENT SOUTH UNIV

Low-melt-viscosity thermosetting polyimide precursor suitable for RTM and preparation method of precursor

ActiveCN110229158AReduce melt viscosityIncrease melt viscosityOrganic chemistryTransfer moldingChemistry
The invention relates to a low-melt-viscosity thermosetting polyimide precursor suitable for resin transfer molding (RTM) and a preparation method of the precursor. The method comprises the followingsteps: commercial binary acid anhydride is used as a basic monomer unit, the commercial binary acid anhydride is combined with a plurality of active monomers to prepare a diaminobisimide macromonomer,the diaminobisimide macromonomer is used as diamine to react with a monoanhydride compound containing a carbon-carbon unsaturated bond, imidization is performed, and therefore the imide oligomer having low melt viscosity, a polymerization degree of 1 and a molecular weight distribution index of 1 is obtained. According to the preparation method provided by the invention, the thermosetting polyimide precursor prepared by the method has a thermal decomposition temperature of higher than 500 DEG C, the melt viscosity of 0.3-0.6 Pa*s, and a resin processing window temperature range from 80 DEG Cto 160 DEG C, can satisfy requirements of the RTM process; and the design idea proposed by the invention can provide technical support for mass production of aerospace polyimide resin composite materials, and provides a possibility for further deepening a wide application of thermosetting polyimide in the field of aerospace.
Owner:NORTHWESTERN POLYTECHNICAL UNIV
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