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19 results about "Sodium salt" patented technology

While sodium is a component of salt, they are not one in the same. In fact, sodium is a mineral found naturally in almost all foods.

Heptatridecafluorooctylpropyl polyhedral oligomeric silsesquioxane and functionalized derivates thereof

InactiveCN103183702AHigh puritySimple processSilicon organic compoundsSilanesEvaporation
The invention provides a preparation method for heptatridecafluorooctylpropyl polyhedral oligomeric silsesquioxane and functionalized derivates thereof. The preparation method comprises the steps as follows: adding tridecafluorooctylpropyl trimethoxy silane into an organic solvent, adding de-ionized water and NaOH, heating, stirring, reacting under reflux condition, washing by a washing solvent, and drying to obtain trisilanol sodium salt of heptatridecafluorooctylpropyl polyhedral oligomeric silsesquioxane; and adding trisilanol sodium salt into an organic reagent, dropwise adding hydrochloric acid, triethylamine and a silane coupling agent, stirring a mixture at normal temperature for reaction, removing generated deposit, carrying out rotary evaporation, removing the solvent, obtaining white crystals, dissolving the crystals in methanol, filtering for collecting insoluble parts, and carrying out vacuum drying to obtain a T8-type monofunctional tridecafluorooctylpropyl POSS (polyhedral oligomeric silsesquioxane) monomer. The preparation method can obtain long branch chain type active fluorine-containing POSS, is simple and easy in process, low in cost, high in yield and higher in product purity, and is suitable for large-scale industrial production.
Owner:HOHAI UNIV

Preparation method of chitosan modified desulfurization adsorbent and application of chitosan modified desulfurization adsorbent in transformer oil treatment

ActiveCN112058243AStrong desulfurization abilityImprove adsorption capacityIon-exchange process apparatusOther chemical processesNano copperTransformer oil
The invention provides a preparation method of a chitosan modified desulfurization adsorbent and application of the chitosan modified desulfurization adsorbent in transformer oil treatment. The preparation method comprises the following steps of: (1) preparing an intermediate hydroxypropyl trimethyl ammonium chloride; (2) preparing a nano copper-loaded adsorbent; (3) preparing a chitosan sodium salt; and (4) modifying the nano copper-loaded adsorbent by chitosan. The self-made chitosan modified desulfurization adsorbent is adopted for adsorption treatment of the transformer oil, the desulfurization rate is high, no pollution is caused, and the desulfurization adsorbent is suitable for deep desulfurization treatment.
Owner:STATE GRID HUBEI ELECTRIC POWER RES INST +2

Sewage pretreatment process used during organic product preparation

ActiveCN109896684APromote precipitationReduce saltOrganic compound preparationMultistage water/sewage treatmentOrganic layerSolvent
An embodiment of the invention discloses a sewage pretreatment process used during organic product preparation. The process includes: (a), adding a nonpolar solvent, sodium alcoholate and main and auxiliary raw materials into a synthesis kettle for reaction; (b), adding a saturated sodium salt solution into a water-washing neutralization kettle, cooling, adding reaction liquid in the synthesis kettle into the water-washing neutralization kettle, and titrating till being slightly acidic; (c), standing a solution in the water-washing neutralization kettle to obtain a lower-layer solid-liquid mixture and an upper-layer organic layer; (d), performing suction filtering on the lower-layer solid-liquid mixture to obtain sodium salt and a mixed solution; (e), taking the mixed solution in the step(d) as the solution added into the water-washing neutralization kettle in the step (b) for reutilization; (f), using water to wash the organic layer, and distilling or rectifying to obtain an organicproduct. The process can promote recycling of sodium salt and reutilizing of sewage, reduce salt in the sewage and substantially lower sewage yield, thereby reducing COD in the sewage and sewage treatment energy consumption and treatment cost.
Owner:ZHANGJIAJIE HONGYAN NEW MATERIAL TECH DEV CO LTD

Stable isotope labeled sulfadoxine and synthesis method thereof

InactiveCN110003120AAtom utilization is highSimple processOrganic chemistry methodsStable Isotope LabelingSynthesis methods
The invention discloses stable isotope labeled sulfadoxine and a synthesis method thereof. The synthesis method comprises following steps: S1, sulfanilamide and sodium hydroxide are subjected to a reaction, and sulfanilamide sodium salt is prepared; S2, sulfanilamide sodium salt and 4,6-dichloro-5-methoxypyrimidine are subjected to a condensation reaction, and 4-sulfanilamide-5-methoxy-6-chloropyrimidine is prepared; S3, 4-sulfanilamide-5-methoxy-6-chloropyrimidine and stable isotope labeled methanol are subjected to an etherification reaction under the alkaline condition, and stable isotope labeled sulfadoxine is prepared. The synthesized stable isotope is high in atom utilization rate, synthesis steps are simple, and a product is easy to separate and purify and meets the requirement of astandard reagent for quantitatively detecting sulfadoxine; stable isotope labeled sulfadoxine has high use value and good economic efficiency.
Owner:SHANGHAI ANPEL SCI INSTR

Method for preparing hemostatic material based on air jet pulverization technology

The invention discloses a method for preparing a hemostatic material based on an air jet pulverization technology. The method comprises the following steps of (1) preparing a fibrinogen solution, wherein the fibrinogen solution comprises the following components of 2.5-3.5 wt% of fibrinogen, 10-25 wt% of trehalose, 2-10 wt% of glycine, 1.0-1.5 wt% of sodium chloride, 0.1-0.6 wt% of sodium citrate, 2.0-2.5 wt% of arginine hydrochloride and the balance of water for injection; (2) performing freeze drying on the fibrinogen solution, and performing air jet pulverization to obtain fibrinogen powder; (3) preparing a thrombin solution, wherein the thrombin solution is prepared from the following components of 0.1 to 0.5 weight percent of thrombin, 1.5 to 5.0 weight percent of trehalose, 0.3 to 1.0 weight percent of calcium chloride, 0.5 to 2.0 weight percent of glycine, 1.0 to 3.0 weight percent of cane sugar, 0.5 to 2.0 weight percent of dextran 20 and the balance of water for injection; (4) performing freeze drying on the thrombin solution, and performing air jet pulverization to obtain thrombin powder; and (5) mixing the fibrinogen powder with the thrombin powder, filling and drying to obtain the hemostatic material. The preparation process is simple, the period is short, and the prepared material is convenient to clinically use and excellent in hemostatic effect and has a wider application prospect.
Owner:FUDAN UNIV

Preparation method of phosphatidylglycerol monosodium salt containing two different side chains

PendingCN111057100AHigh purityHigh yieldPhosphatide foodstuff compositionsPhosphorus organic compoundsSide chainPhospholipid
The invention belongs to the technical field of compound preparation. The invention relates to a preparation method of phosphatidylglycerol monosodium salt, in particular to a preparation method of phosphatidylglycerol monosodium salt containing two different side chains. The preparation method comprises the following steps: taking D-mannitol as an initial raw material, heating D-mannitol in acetone to generate 1,1,5,6-isopropylidene-D-mannitol; carrying out sodium periodate oxidation and sodium borohydride reduction to obtain iso-propylidene glycerol; carrying out condensation reaction with fatty acid containing an R1 element, then removing acetal protective groups in the presence of acid; selectively protecting primary hydroxyl by using a silane protective agent, reacting secondary hydroxyl with another fatty acid containing a R2 element, removing silane protection, reacting the de-protected product with phosphorus oxychloride and iso-propylidene glycerol, removing acetal protectivegroups by using an acid, and finally carrying out a sodium salt treatment to obtain a final product. The synthesis of phosphatidyl monosodium salt containing two different side chains can be realized,and the production process is simple, environment-friendly and easy to operate.
Owner:HEFEI BOSIKC PHARMTECH CO LTD

Fly ash enhanced washing and high-salinity wastewater resource utilization method

PendingCN113953303AAchieve harmlessReach resourcesSolid waste disposalWater contaminantsSaline waterSalt water
The invention discloses a fly ash enhanced washing and high-salinity wastewater resource utilization method. According to the fly ash enhanced washing and high-salinity wastewater resource utilization method, firstly, fly ash is subjected to water bath heating washing, the heating temperature ranges from 50 DEG C to 60 DEG C, a large number of soluble anions and heavy metal ions in the fly ash can be efficiently removed through the water bath heating washing mode, most heavy metal is washed out, and washing liquid and harmless fly ash are obtained; heavy metal precipitates in the washing liquid are removed in an inorganic-organic flocculating agent combined mode, purified high-salt water washing liquid and heavy metal precipitates are obtained, and the total heavy metal removal rate in the washing liquid can reach 99%; and the purified high-salinity water washing liquid contains about 6-15 wt% of potassium and sodium salts, the high-salinity water washing liquid is subjected to evaporative crystallization through an MVR evaporator, potassium salts are obtained through cooling crystallization, the potassium salts and mixed salt waste liquid are obtained through centrifugal separation, the mixed salt waste liquid is electrolyzed to obtain the sodium salts, recovery of the potassium salts and the sodium salts is achieved, and the potassium salt vacancy in China can be relieved.
Owner:JIANGXI GAIA ENVIRONMENTAL SCI & TECH CO LTD +1

Hypsizygus marmoreus culture medium

InactiveCN105036942AShorten the growth cycleIncrease productionFertilizer mixturesSeaweed extractSodium salt
The invention relates to a hypsizygus marmoreus culture medium. The hypsizygus marmoreus culture medium is prepared from the following raw materials: 50-63% of husked millet meal, 28-32% of beech wood chips, 0.1-0.4% of potassium phosphate, 1-2% of lactose, 0.5-1.2% of calcium nitrate, 0.01-0.015% of alpha-naphthylacetic sodium salt, 3.5-4% of a seaweed extract, 3-7% of crab shell powder and 1-3 parts of molasses. The hypsizygus marmoreus culture medium can shorten the growth cycle of hypsizygus marmoreus, the mycelium permeates 18-20 days after the hypsizygus marmoreus culture medium is inoculated with hypsizygus marmot reus strain as a substrate, pollution microbes are prevented in the culture period, and both the yield and the quality of hypsizygus marmoreus can be remarkably improved.
Owner:HEFEI YUANZHENG AFE SCI TECH
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