The invention relates to the technical field of
ammonia distillation processes, in particular to a method for controlling the liquid caustic soda addition amount in an
ammonia distillation process based on
conductivity change, and solves the problem of control of the liquid caustic soda addition amount in the
ammonia distillation process. The method for controlling the liquid caustic soda addition amount in the ammonia distillation process based on the
conductivity change comprises the following steps: 1, gradually adding liquid caustic soda into an
ammonium sulfate solution in a dropwise manner, determining and recording the pH value change of the solution, the
conductivity change of the solution and the liquid caustic soda input amount in the whole process of adding the liquid caustic soda; 2, after the
ammonium sulfate solution and the caustic soda liquid are mixed to reach a reaction equivalent point, continuously adding the caustic soda liquid into the
mixed solution, and continuously determining the pH value of the solution, the conductivity of the solution and the addition amount of the caustic soda liquid. According to the invention, two
ammonium sulfate solutions with different concentrations and a
sodium hydroxide solution are adopted to carry out a variable control experiment, and the method for controlling the liquid caustic soda addition amount in the ammonia distillation process based on the conductivity change is provided according to the change relationship between the solution conductivity and the liquid caustic soda addition amount in the ammonia distillation process.